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Metrology
MetrologyInstrumentation

STA 319 Jupiter

By NETZSCH-Geratebau GmbH

Simultaneous Thermal Analysis generally refers to the simultaneous application of Thermogravimetry (TGA) and Differential Scanning Calorimetry (DSC) to one and the same sample using a single instrument. The advantages are obvious. For a single sample, the TGA and DSC signals can be obtained under perfectly identical experimental conditions, including: - Atmosphere - Gas flow rate - Vapor pressure on the sample - Heating rate - Thermal contact with the sample crucible - Sensor radiation effect, etc. Furthermore, sample throughput is improved as more information can be gathered from each test run. DSC Possibilities - Melting/crystallization behavior - Solid-solid transition - Glass transition - Oxidative stability - Specific heat capacity - Degree of crystallinity - Cross-linking reactions - TM-DSC - Kinetics simulations TGA Possibilities - Mass changes - Decomposition - Oxidation/reduction behavior - Temperature stability - Compositional analysis - Corrosion studies - Kinetics simulations TOP-LOADING DESIGN FOR FREE AND SAFE ACCESS ADVANCED MICROBALANCE FOR ACCURATE TGA RESULTS HIGH-PERFORMANCE DSC SENSOR FOR RELIABLE AND PRECISE RESULTS LARGE AUTO SAMPLER AND COUPLING OPTIONS FOR HIGH EFFICIENCY AND ANALYTICAL DEPTH VACUUM-TIGHT DESIGN FOR DEFINED ATMOSPHERIC CONDITIONS FAST THERMAL CONTROL VIA SOPHISTICATED FURNACE Explore the STA 319 Jupiter: Furnace heater Furnace Furnace water cooling Sample carrier Sample holder lifting device Balance Purge gas sample Thermostatic control balance Protective gas balance chamber Gas outlet Sample and crucible Sensor Radiation shield Quick connector with ID sensor Innovative Design. Uncompromised Precision – the New DSC-TGA Sample Carrier The STA 319 Jupiter DSC-TGA sample carrier features a reference ring design that replaces the conventional reference crucible. This design simplifies handling, provides a stable thermal reference point, and improves measurement consistency, resulting in more reliable experimental outcomes. Innovative Balance Design for Reliable Results Achieve outstanding accuracy and reproducibility with a top-loading microbalance that delivers a 20-ng resolution as well as clean and stable baselines. During sample loading, the balance is automatically decoupled via the hoisting mechanism, reducing mechanical influence on the microbalance and preventing potential damage. Robust and Fast-acting Furnace The low-volume furnace enables rapid heating and ballistic cooling from 1100°C to room temperature, saving time and improving efficiency. Magnetic Shock Absorbers in the Device Base The standard feet on the STA 319 Jupiter series can be optionally replaced with a patented magnetic levitation system (Patent DE 10 2020 007 279 B4; US 11,747,176 B2) that effectively shields the instrument from external disturbances such as vibration. This feature provides reliable results that are unaffected by environmental impact. Technical Specifications Design Top-loading Instrument interface Touch display Temperature range (10°C) RT to 1025°C/1100°C Heating rate 0.001 K/min to 300 K/min Cooling time - In nitrogen: ≈ 12 min from 1100°C to 100°C - In helium: ≈ 5 min from 1100°C to 100°C, ≈10 min to 25°C Max. sample weight/measuring range 2 g Balance resolution 20 ng TGA accuracy 0.0003% DSC accuracy ± 5% Temperature resolution 0.001 K Temperature accuracy ± 0.3 K (after calibration by DSC/c-DTA, indium) Temperature precision 0.15 K Temperature calibration - DSC/c-DTA, also for detection of endo- and exothermal effects - TGA calibration - Curie calibration Vacuum-tightness < 10 -1 mbar AutoVac Automatic evacuation and refilling of purge gas; optionally available when MFC is selected Gas control (optional) - Gas switch - integrated 3-fold MFC - integrated 4-fold MFC Evolved Gas Analysis Optional 192+12-position ASC Optional Piercing device Optional Unlimited Warranty Optional

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