By Department of Nanoscale Science & Engineering, University at Albany
INSTRUMENTAL CHARACTERISTICS SPECTROMETER - Two channels console. - Fully automatic autotune and matching control of all nuclei in the probe range. - 200W High Frequency Power Amplifier: 550 to 610 MHz. - 500W Low Frequency Power Amplifier: 5 to 245 MHz. - Matrix shim system, shim controller, shim driver and shim coil. - Automatic and manual shimming. - Variable temperature control, temperature range: from -170 to 250°C. - Computer driven air controller for sample loading and spinning SUPERCONDUCTOR MAGNET 600 MHz - 14.09 Tesla magnetic field. - Low cryogenic consumption. Cryogenic liquid level meter (helium and nitrogen). - High efficiency anti-vibration system specific for the magnet. - High efficiency external noise suppression system (≥99%). 600 MHz 5 mm FG/RO DIGITAL AUTOTUNE PROBE - 5 mm high sensitivity ROYAL HFX NMR probe - Coils optimized for proton, fluorine, and multinuclear observation and decoupling - Observable and irradiable nuclei: 1H, 19F, from 31P to 15N. - Digital auto-tune and match ready, Z-axis pulsed field gradient coil, 2H lock. - Provides 1H{19F}, 19F{1H}, 13C,{1H,19F}, and X{1H,19F} experiments with switchable magnet idler coil tuning and no performance loss in standard 1H or 19F mode.. - Coils optimized for proton, fluorine, and multinuclear observation and decoupling, heteronuclei selection by software. - Variable Temperature operation: from -100 to + 150°C. 600MHZ 10MM LOW FREQUENCY TUNABLE PROBE - 10 mm high sensitivity broadband low frequency probe. - Optimized for low frequency multinuclear observation with 1H decoupling, - 2H lock. - Nuclei include: 1H, 15N to 103Rh. - Variable Temperature operation from -50° C to +120° C. 600MHz 3.2MM HX AUTOMAS PROBE, TOP LOADING - AUTOMAS probe and ROTOCARRIER bring the usability of solution NMR probe to solid-state NMR spectroscopy. - Probe has the automatic tuning function, all operations including sample loading, sample spinning, temperature control, probe tuning and experimental can be done in fully automated way. - Solution and solid-state probes can share the same auto sample charger. - High Temperature Solids VT Adapter. VT range: Ambient to +200° C. - Low Temperature Solids VT Adapter. VT Range: -100° C to ambient. - JEOL 3.2 mm bench spinner for sample spin testing. Maximum spinning speed 21 KHz. - 3.2mm solid sample tool kit - Includes tools for packing and unpacking 3.2 mm Magic Angle Spinning (MAS) rotors. - 3.2mm zirconia sample tubes - variable temperature use, -100° C to +150° C. Max speed 22KHz, sample volume 49µL. WORKSTATION - Dell Precision Workstation / Windows 10 64-Bit. - JEOL "Flex Automation" automated 'point and click' NMR operation software with automatic gradient shimming, user-defined automation and data presentation - 3.0 GHz (4.4 GHz Turbo) 6 Core CPU, 16 Gbyte RAM, 1 Tbyte disk drive - 2 Gbyte color graphics card, 24" color flat screen display, DVD+/-RW drive, alphanumeric keyboard, optical mouse. DATA MANAGEMENT SYSTEM - Comprehensive Delta FT-NMR Software including 1, 2, 3-D data acquisition, processing, display, and plotting. - JEOL "Flex Automation" automated 'point and click' NMR operation software with automatic gradient shimming, user-defined automation and data presentation - Macro programming language - DOSY data analysis and presentation.
